. Reflux Still Instructions

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Make the highest quality Distillates at home!

Use a reflux Still!

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 how to make a alcohol still

Small Still Engineering L.L.C. has licensed me to distribute these Copyrighted Documents!

 

This a guide on how you can construct your own sophisticated distillation apparatus called a reflux still, they are not plans for a pot still (Which are more dangerous and produce a lower quality product See below!). reflux still colum “It is directed at anyone who may want to know more about the subject, for hobbyists, tinkers, pure water enthusiasts, survivors, and perhaps amateur wine and beer makers.” The guide is for an advanced reflux still that uses the different boils points of liquids to separate out one in a pure form or what is called a “single batch”. Next a compact water-jacketed condenser cools the distillate back into a liquid, which can then be captured. 

Although this guide is over 30-page and for a sophisticated reflux distillation apparatus it is friendly, easy to follow, and has step-by-step instructions with many pictures. The guide “mixes how the still is built with why it’s being built that way” to “provide enough background to allow someone to make fine adjustment to the design to better suite their needs”. The document was copyrighted by Small Still Engineering LLC in1999. The construction of this unite is manageable for anyone who is handy, mostly cutting pipe and soldering or welding. You build this at home! Most of the parts can even be purchased at a local hardware or plumbing supply store (the other parts n Ebay) for a little more than a hundred dollars. Include with the instructions are safe operating guidelines, recipes for different kinds of spirits and related web pages. The reflux still apparatus can be used for distilling either water or alcohol. “At the time of this writing [of the guide], there is only one like it.”

Learn about the distillation of alcohol with this powerful guide!

You have to check these out before spending hundreds of dollars on a less sophisticated still! 

 

 

  If you’re thinking about buying a pot still, or the instructions to build, one read these quotes from our guide first

 

 

Making distilled spirits:

  • "The problem with pot stills is that they don’t do a good job at separating out exactly what you want to distill as output. They are usually used to separate compounds whose boiling points differ by about 100º C. When fermented liquid is distilled, lots of things come out, some good, some bad. And because there are no fine controls on this kind of still, the output contains a lot of impurities. Nevertheless, after each distillation, you always get a better output product from that which you started with. So each time you redistill the output in a pot still, it will come out a bit purer, but you lose a little each time you redistill. To make it really pure, you have to distill it so many times that you’ll end up with almost no output. If you don’t re-distill the output several times, you can get a massive hangover by drink whatever comes out. Hangovers are caused by the impurities in the alcohol. In short, you’ve been poisoned (but just a little bit)!”

 

  • “Basically, the reflux still is a structure that allows the distillate vapors from a boiler to rise up a column to the top where the vapors are condensed. The condensed liquid is then allowed to run back down through the rising vapors to a point where the temperatures become hot enough that it boils again. This process is called refluxing. As this cycle continues, the mixture inside the tower is effectively re-distilled. In the process, the components of the mixture separate into discrete layers within the column based on their boiling points.” “At the time of this writing, there is only one like it.”

 This is the same way it is done in industry, except their stills allow them to draw off  the multiple layers, or different chemical components, at once!

 

More peaces:

 

  • The pages that follow contain a step by step guide to building a relatively sophisticated still. It is directed at anyone who may want to know more about the subject, for hobbyists, tinkers, pure water enthusiasts, survivors, and perhaps amateur wine and beer makers. The still involved in the chapters that follow is a unique distillation apparatus. At the time of this writing, there is only one like it. Designing and building this apparatus is the only subject of this manual and you will find that it confines itself to those areas. It does not enter into the domains of fermentation, recipes for making mash, beer, wine or any other spirits. These areas are covered in detail in other readily available books and numerous web sites.

 

  • Everyone should follow his or her own conscience in these matters.” “So, as long as your conscience allows, at least in the US, you are not doing anything wrong by reading this information. There is also nothing illegal about building a still.”

 

  • In the US (and many other countries) you know that doing that is just not the politically correct thing to do. Even if you are just a curious person and simply want to know what’s involved, you probably feel some reluctance about discussing the subject outside of your own trusted circles. The reason you feel this way, most likely, is because a lot of laws have been passed over time that severely restrict the ways that you may refine products containing ethyl alcohol. Most US residents are also quite familiar with the moonshine folklore, high-powered cars running moonshine over mountain back roads, and dodging the federal revenue agents. So much so that many may feel that they are doing something improper, or maybe even criminal by reading this. Everyone should follow his or her own conscience in these matters. Personally, I believe that some of these laws are so poorly thought out and implemented that they border on being ridiculous. 

 

  • A case in point, in the US, the government allows an individual to produce wine or beer for personal consumption by using a fermentation process to produce an alcoholic beverage. The fermentation process however, produces a wine or beer containing chemicals that are actually poisonous for human consumption. Nevertheless, the government seems to think it is perfectly OK for an individual to ferment and drink the stuff, regardless of the impurities it may contain. Unbelievably, the US government also makes it illegal for an individual to remove the poisons from the alcohol in the wine or beer by distillation. In other words, it is illegal for an individual to refine a legal beverage in their own home and, in the process, produce another perfectly legal beverage for their own consumption! Figure that one out.  Without much reflection, it is easy to see that such laws are flawed and without foundation in logic, justice, or the common good.

 

  • Fortunately, it is not illegal to express these opinions. That freedom also extends to writing about such things as alcohol distillation (legal or not), and the use and manufacture of equipment to effect this process in the home. There is also nothing illegal about building a still. Having said that, recognize that the only purpose of this document is to educate and inform those of you who are interested in this subject. It is not to be construed in any fashion as an encouragement to break the law. If you believe the law is incorrect, please take the time to contact your representatives in government, cast your vote at the polls, write newsletters to the media, and in general, try to make the changes in a legal and democratic manner.”

   

 

 

 

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The guide is not only filled with color pictures, but color diagrams like this that show exactly how this reflux still is constructed!

A diagram from our complete guide!

 

Below is the written instruction for this diagram!

--some parts of the below have been deleted or altered.

 

The reflux column is the tube that runs straight up from the top of the boiler. The column is made from xx" copper tubing, is about xxx feet long,  It is packed with "Raschig" rings (described later) to provide a large area condensation surface inside the column, and it has two cooling tubes that pass water through the vapors that rise through the column from the boiler. It also has a  connection at the top to accommodate a condenser, and a screen at the bottom to keep the packing from falling out. The column head section consists of a cap, a thermometer, a xx" long nipple, and a connector. It also includes a connection to the condenser assembly with two xx" x xx" nipples, and a xx" elbow. A drawing of the assembly is shown above:

 

 

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Picture of entire reflux Still!

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